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Synthesis of large quantities of single-walled aluminogermanate nanotube

Levard C., Rose J., Masion A., Doelsch E., Borschneck D., Olivi L., Dominici C., Grauby O., Woicik J.C., Bottero J.Y.. 2008. Journal of the American Chemical Society, 130 (18) : p. 5862-5863.

DOI: 10.1021/ja801045a

A simple aqueous synthesis yielded about 100 times more structurally well-organized single-walled aluminogermanate nanotubes than previously reported "standard" procedures. The structure analyses using XRD, IRTF, TEM, and XAS were greatly facilitated by the high concentrations available, and they ascertained the imogolite-like structure of the nanotubes. Simplicity and yield of the synthesis protocol are likely to favor commercial applications of theses materials as well as simplified syntheses of other nanophases.

Mots-clés : synthèse chimique; structure chimique; cylindre; silicium; aluminium; nanotube

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